Ano do artigo | 2020 |
Descrições/informações adicionais | Polymers synthesized by molecular imprinting technology are commonly known as molecularly imprinted polymers (MIP). In this work, nanoparticles of MIP for β-caryophyllene (NP-MIP-βCP) were synthesized and incorporated into poly (ε-caprolactone) PCL fibers by electrospinning, where morphological characterization was performed by SEM and average diameter of 129 ± 32.3 nm was found. Also, PCL electrospun fiber diameters without and with nanoparticles were 1.66 ± 1.12 and 0.70 ± 0.24 µm, respectively. Chemical characterization by infrared spectroscopy (FTIR) confirmed the synthesis of the NP-MIP-βCP and vibrational band present at 1628 cm-1 indicates the insertion of the NP-MIP-βCP into PCL fibers. It was found the influence of the incorporation of NP-MIP-βCP in thermal and tensile properties of the PCL electrospun membrane. Therefore, NP-MIP-βCP can be incorporated in PCL electrospun membranes by electrospinning and presents a potential application in the pharmaceutical and biomedicine areas, and biosensors. |
Descrições/informações adicionais(EN) | Polymers synthesized by molecular imprinting technology are commonly known as molecularly imprinted polymers (MIP). In this work, nanoparticles of MIP for β-caryophyllene (NP-MIP-βCP) were synthesized and incorporated into poly (ε-caprolactone) PCL fibers by electrospinning, where morphological characterization was performed by SEM and average diameter of 129 ± 32.3 nm was found. Also, PCL electrospun fiber diameters without and with nanoparticles were 1.66 ± 1.12 and 0.70 ± 0.24 µm, respectively. Chemical characterization by infrared spectroscopy (FTIR) confirmed the synthesis of the NP-MIP-βCP and vibrational band present at 1628 cm-1 indicates the insertion of the NP-MIP-βCP into PCL fibers. It was found the influence of the incorporation of NP-MIP-βCP in thermal and tensile properties of the PCL electrospun membrane. Therefore, NP-MIP-βCP can be incorporated in PCL electrospun membranes by electrospinning and presents a potential application in the pharmaceutical and biomedicine areas, and biosensors. |
Divulgação científica | NAO |
DOI | 10.1016/j.matlet.2020.128088 |
Homepage do trabalho | [http://https://www.sciencedirect.com/science/article/pii/S0167577X2030793X?dgcid=coauthor] |
Idioma | Português |
ISSN | 0167577X |
Meio de divulgação | MEIO_DIGITAL |
Natureza | COMPLETO |
Página inicial | 128088 |
Relevânica | NAO |
Sequencia da produção | 157 |
Série | 15 |
Título do artigo | Incorporation of Molecularly Imprinted Polymer Nanoparticles in Electrospun Polycaprolactone Fibers |
Título do artigo(EN) | Incorporation of Molecularly Imprinted Polymer Nanoparticles in Electrospun Polycaprolactone Fibers |
Título do periódico ou revista | MATERIALS LETTERS |
Volume | 275 |